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Beilstein J. Org. Chem. 2010, 6, 1120–1126, doi:10.3762/bjoc.6.128
Graphical Abstract
Figure 1: Representative olefin metathesis catalysts.
Figure 2: Highly active olefin metathesis catalysts bearing NHC with backbone substitution.
Scheme 1: Synthesis of the free NHCs.
Scheme 2: Synthesis of [RhCl(CO)2(NHC)] complexes.
Scheme 3: Synthesis of [RuCl2(NHC)(PCy3)(Ind)] complexes.
Beilstein J. Org. Chem. 2010, 6, 1091–1098, doi:10.3762/bjoc.6.125
Figure 1: General layout for modifications of ruthenium-based olefin metathesis catalysts (red: anionic ligan...
Scheme 1: Synthesis of 1, 2 and 3.
Figure 2: Details of the 1H NMR spectra acquired during the synthesis of 2 and the FD-MS spectrum of 2 isolat...
Figure 3: ORTEP drawing of 3. Thermal ellipsoids are drawn at 50% probability level. Hydrogen atoms are omitt...
Figure 4: Polymerisation of 4 as a function of time, initiated by 1, 2 or 3, monitored by 1H NMR spectroscopy...
Figure 5: Polymerisations of 6 as a function of time, initiated by 1–3, monitored by 1H NMR spectroscopy (sol...
Figure 6: The RCM reaction of 7 as a function of time, catalysed by 1, 2 or 3, monitored by 1H NMR spectrosco...